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...Activity cite this j chem educ pubs acs org jchemeduc inquiry based experiment with powder xrd and fes crystal discovering the peak n stojilovic d e isaacs department of physics astronomy chemistry university wisconsinoshkosh oshkosh wisconsin united states s supporting information abstract we discuss how a x ray diraction system can be used to probe large pyrite crystals reveal generally not documented in literature ability detect is attributed use which gives signal intensities type provides research like experience students opportunity deepen their understanding orders are rst challenged creative determine mount mineral then practice critical thinking order origin unknown may also generalized other than keywords upper division undergraduate physical discovery learning solid state student centered crystallography introduction missing peaks preferred orientation they traditional laboratories often instructed on what comparing an pattern single that measure thus do fully develop try gu...