nitrogen determination by kjeldahl method nitrogen determination by kjeldahl method the kjeldahl method is used to determine the nitrogen content in organic and inorganic samples for longer than 100 years ...
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...Nitrogen determination by kjeldahl method the is used to determine content in organic and inorganic samples for longer than years has been of a wide range made foods drinks meat feeds cereals forages calculation protein also wastewaters soils other it an official described different normatives such as aoac usepa iso din pharmacopeias european directives procedure involves three major steps digestion distillation titration nh distilled converted into determined retained receiver vessel aim break all bonds sample convert organically bonded ammonium ions carbon hydrogen form dioxide water this process material carbonizes which can be visualized transformation black foam during decomposes finally clear liquid indicates completion chemical reaction purpose mixed with sulfuric acid at temperatures between c higher temperature faster obtained speed greatly improved addition salt catalysts potassium sulfate added order increase boiling point are efficiency oxidizing agents improve even further...